Sökning: "SEM EDX"

Visar resultat 1 - 5 av 66 avhandlingar innehållade orden SEM EDX.

  1. 1. Microscopy of high temperature oxidation of iron and some stainless steels

    Författare :Torbjörn Jonsson; Chalmers University of Technology; []
    Nyckelord :water vapour; sulphur dioxide; FIB; X20; stainless steel; 353MA; EDX; KCl; FIB SEM; SEM; microstructure; TEM; iron; High-temperature oxidation; in-situ ESEM;

    Sammanfattning : This thesis concerns the high temperature oxidation of iron and some stainless steels. The oxide scales, as well as the subjacent metal, were investigated using a range of electron and ion microscopy techniques, including SEM, TEM, EDX and FIB. The aim was to link the microstructural observations to the oxidation mechanisms of the materials. LÄS MER

  2. 2. Microscopy investigation of the high temperature corrosion of iron and two stainless steels

    Författare :Torbjörn Jonsson; Chalmers University of Technology; []
    Nyckelord :353MA; EDX; X20; TEM; stainless steel; water vapour; iron; SEM; vaporisation; High-temperature oxidation; microstructure; FIB SEM.; sulphur dioxide; FIB;

    Sammanfattning : .... LÄS MER

  3. 3. Microstructure of Zirconium Alloys Oxidized in Steam

    Författare :Pia Tejland; Chalmers University of Technology; []
    Nyckelord :TEKNIK OCH TEKNOLOGIER; ENGINEERING AND TECHNOLOGY; EDX; ADF; TEM; Zircaloy-2; FIB-SEM; STEM; GD-OES; SPP; SEM; Zirconium; HAADF;

    Sammanfattning : Zirconium alloys are widely used in nuclear reactors as fuel cladding tubes because of their low thermal neutron capture cross-section, good corrosion properties and satisfactory mechanical properties. However, the main limiting factor of these materials is the oxidation behavior. LÄS MER

  4. 4. Atmospheric corrosion of Mg and MgAl alloys – characterization and mechanisms

    Författare :Mehrdad Shahabi Navid; Chalmers University of Technology; []
    Nyckelord :TEKNIK OCH TEKNOLOGIER; TEKNIK OCH TEKNOLOGIER; ENGINEERING AND TECHNOLOGY; ENGINEERING AND TECHNOLOGY; EDX; CO2; XPS; Mg and MgAl alloys; NaCl; Atmospheric corrosion; Characterization; 3D imaging; SEM; BIB; Thin film; FTIR; XRD; Pitting; Interference microscopy; FIB;

    Sammanfattning : The atmospheric corrosion of Mg and MgAl alloys was investigated. Corrosion tests were performed in the laboratory under controlled environment. CP Mg, AM50 and AZ91 samples were exposed at 95% RH and 22°C in the presence and in the absence of 400 ppm CO2 for 24 h to 672 h. The passive film was characterized by means of XPS, FTIR, AES and XRD. LÄS MER

  5. 5. Microstructure of a cubic boron nitride tool material before and after hard turning

    Författare :Jenny Angseryd; Chalmers University of Technology; []
    Nyckelord :TEKNIK OCH TEKNOLOGIER; ENGINEERING AND TECHNOLOGY; EELS; cBN; microstructure; PCBN; adherent layer; EDX; wear; SEM; EFTEM; TEM;

    Sammanfattning : AbstractPolycrystalline cubic boron nitride (PCBN) materials are widely used in turning of hardened steels due to their beneficial mechanical properties like high hardness at elevated temperatures and, compared to diamond, for being more chemically stable towards iron at temperatures typical for turning operations (800-1000˚C). The wear of PCBN tools is influenced by several factors, like machining parameters, different tool geometries and varying composition of PCBN tools as well as workpiece material. LÄS MER